CHM443A - Inorganic Chemistry Lab
Prerequisites:
0-0-6-6
Course Contents
Invisible ink .
Utilization of coordination chemistry to demonstrate invisible ink in laboratory
Color effects due to ligand-exchange in nickel complexes
Demonstration of ligand-field strength in the spectrochemical series
Color effects in aqueous systems containing divalent 3d metal ions
Demonstration of crystal-field splitting parameters of 3d metal ions
Acidic and basic salts
Hydrolysis of salts and its consequences
Preparation of nitro- and nitrito-pentamminecobalt(III) chloride
Linkage isomers: synthesis and identification using various spectroscopic techniques
The preparation of hexamminecobalt(III) chloride and pentammineaquocobalt(III) chloride
Synthesis, isolation and characterization of the complex
The preparation of cis-and trans -potassiumdioxalatodiaquochromate(III)
Geometrical isomers: synthesis and identification using various spectroscopic techniques
Aquation oftrans-dichloro-bis(1,2-diamminoethane)cobalt(III)chloride
Investigation of acid hydrolysis of the complex
The preparation and resolution of tris(ethylenediamine)cobalt(III)ion into its optical antipodes
Optical isomers: synthesis, isolation and characterization
Preparation of hexamminenickel(II) chloride: estimation of ammonia and nickel by titrimetric and gravimetric methods
Determination of complex composition using simple techniques
Synthesis and reactions of organo cobaloximes
Synthesis of an air-sensitive organometallic complex at low temperature under inert atmosphere
Synthesis and characterization of ferrocene and acetylferrocene
Synthesis, purification using chromatography and characterization
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